Assessment of particle size distribution and tensile properties of hybrid epoxy composite reinforced with functionalized graphene and CNT nanofillers

Shukla, Manoj Kumar; Sharma, Kamal

doi:10.22061/jcarme.2022.5312.1656

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	Assessment of particle size distribution and tensile properties of hybrid epoxy composite reinforced with functionalized graphene and CNT nanofillers
Journal of Computational & Applied Research in Mechanical Engineering (JCARME)
مقاله 1، دوره 12، شماره 1 - شماره پیاپی 23، آبان 2022، صفحه 1-12 اصل مقاله (594.25 K)
نوع مقاله: Research Paper
شناسه دیجیتال (DOI): 10.22061/jcarme.2022.5312.1656
نویسندگان
Manoj Kumar Shukla^* ¹؛ Kamal Sharma²
¹Department of Mechanical Engineering, Institute of Engineering & Technology, GLA University, Mathura 281406, India, Kalaniketan Polytechnic College, Jabalpur 482001, Jabalpur, Affiliated to Rajiv Gandhi Technical University, Bhopal, India
²Department of Mechanical Engineering, Institute of Engineering & Technology, GLA University, Mathura 281406, India
تاریخ دریافت: 01 خرداد 1398، تاریخ بازنگری: 14 فروردین 1401، تاریخ پذیرش: 15 فروردین 1401
چکیده
The synergetic effect of amine functionalized multiple graphene layers (AMGL) and multi-walled carbon nanotube (AMWCNT) nano-fillers mixed with epoxy resin is investigated on the particle size distribution (PSD) and tensile properties of hybrid composites. The hybrid composites with an equal ratio of nano-fillers at a weight percent of 0.25, 0.50, 1, and 2 wt % are fabricated. The particle size analysis (PSA) is performed by the dynamic light scattering (DLS) technique and image analysis (IA) method; both verify PSD for composites. This is further verified by the analyses of scanning electron microscopy (SEM) images using Image J software. The optimum composite particle size of 6.8 µm and homogeneous mixture with a poly-dispersity index (PI) of 0.74 is investigated for a sample having filler content of 0.5 wt %. Tensile stress and elastic modulus is also found to be maximum at 0.5 wt %, which is 49.91 MPa of 2302 Mpa, respectively. The chemical composition of composite affecting its PSD is characterized by energy dispersive X-ray (EDX) process. Dimensional analysis of particle size in the domain of epoxy matrix provides deep insights to the researchers and may also provide them a direction for selecting an appropriate material for a particular application.
کلیدواژه‌ها
Particle size distribution؛ Hybrid composite؛ Image analysis؛ Tensile strength؛ Elastic modulus

مراجع
[1] A. Kumar and K. Sharma, “A review of the mechanical and thermal properties of graphene and its hybrid polymer nanocomposites for structural applications,” J. Mater. Sci., Vol. 54, No. 8, pp. 5992–6026, (2018). [2] A. K. Geim and K. S. Novoselov, “The rise of graphene.,” Nat. Mater., Vol. 6, No. 3, pp. 183–91, (2007). [3] E. Thostenson, “Advances in the science and technology of carbon nanotubes and their composites: a review,” Compos. Sci. Technol., Vol. 61, No. 13, pp. 1899–1912, (2001). [4] V. Singh, D. Joung, L. Zhai, S. Das, S. I. Khondaker and S. Seal, “Graphene based materials: Past, present and future,” Prog. Mater. Sci., Vol. 56, No. 8, pp. 1178–1271, (2011). [5] Y. J. Wan, “Grafting of epoxy chains onto graphene oxide for epoxy composites with improved mechanical and thermal properties,” Carbon N. Y., Vol. 69, No. November, pp. 467–480, (2014). [6] G. Zhang, F. Wang, J. Dai and Z. Huang, “Effect of functionalization of graphene nanoplatelets on the mechanical and thermal properties of silicone rubber composites,” Materials (Basel)., Vol. 9, No. 2, p. 92, (2016). [7] P. K. Singh and K. Sharma, “Mechanical and Viscoelastic Properties of In-situ Amine Functionalized Multiple Layer Grpahene / epoxy Nanocomposites,” Curr. Nanosci., Vol. 14, No. 6, pp. 252–262, (2018). [8] J. Wang, “Graphene and Carbon Nanotube Polymer Composites for Laser Protection,” J. Inorg. Organomet. Polym. Mater., Vol. 21, No. 4, pp. 736–746, (2011). [9] C. Hadden, “Mechanical Properties of Graphene Nanoplatelet / Carbon Fiber / Epoxy Hybrid Composites : Multiscale Modeling and Experiments,” Carbon N. Y., Vol. 95, No. July, pp. 100–112, (2015). [10] Z. Ghaleb and A. Z. Mariatti M, “Synergy effects of graphene and multiwalled carbon nanotubes hybrid system on properties of epoxy nanocomposites,” J. Reinf. Plast. Compos., Vol. 36, No. 9, pp. 685–695, (2017). [11] M.T. Le and S.C. Huang, “Thermal and Mechanical Behavior of Hybrid Polymer Nanocomposite Reinforced with Graphene Nanoplatelets,” Materials (Basel)., Vol. 8, No. 8, pp. 5526–5536, (2015). [12] U. Szeluga, B. Kumanek and B. Trzebicka, “Synergy in hybrid polymer/nanocarbon composites. A review ” Compos. PART A, Vol. 73, No. November, pp. 204–231, (2015). [13] F. Liu, “Investigation on the interfacial mechanical properties of hybrid graphene-carbon nanotube/polymer nanocomposites,” Carbon N. Y., Vol. 115, pp. 694–700, (2017). [14] G. I. Giannopoulos and I. G. Kallivokas, “Mechanical properties of graphene based nanocomposites incorporating a hybrid interphase,” Finite Elem. Anal. Des., Vol. 90, pp. 31–40, (2014). [15] M. K. Shukla, A. Kumar, A. Yadav and K. Sharma, “Improved Mechanical Properties of Graphene Oxide Reinforced Cross-linked Epoxy Nanocomposites: A Molecular Dynamics Approach,” Mater. Today Proc., Vol. 11, No. 2, pp. 679–685, (2019). [16] M. K. Shukla, A. Yadav, A. Kumar and K. Sharma, “Investigating the Effects of Amine Functionalized Graphene on the Mechanical Properties of Epoxy Nanocomposites,” Mater. Today Proc., Vol. 11, No. 2, pp. 837–842, (2019). [17] P. J. Lu, “Methodology for sample preparation and size measurement of commercial ZnO nanoparticles,” J. Food Drug Anal., Vol. 26, No. 2, pp. 628–636, (2018). [18] B. Zewde, P. Pitliya, A. Karim and D. Raghavan, “Synergistic Effect of Functionalized Carbon Nanotubes and Micron-Sized Rubber Particles on the Mechanical Properties of Epoxy Resin,” Macromol. Mater. Eng., Vol. 301, No. 5, pp. 542–548, (2016). [19] Y. Zhou, E. White and S. Jeelani, “Effect of particle size on the mechanical properties of polymer matrix nanocomposite,” Materials Science,Vol. 1, pp. 316–319, (2007). [20] S. K. Bhattacharyya and S. Basu, “Effect of particle size on the mechanical properties of poly ( vinylchloride ) -copper particulate composite,” Mater. Sci., Vol. 13, pp. 2109–2118, (1978). [21] V. M. Dalfard, “Effect of particle size of tungsten carbide on weight percent of carbide in Ni-WC nano-composite,” Int. J. Electrochem. Sci., Vol. 7, No. 4, pp. 3537–3542, (2012). [22] J. Ruzic, K. Jakimovska, N. Stoimenov, S. Gyoshev and D. Karastoyanov, “Influence of mechanical alloying time on particle size of copper matrix composite,” Journal of Achievements in Materials and Manufacturing Engineering, Vol. 68, No. 2, pp. 53–58, (2015). [23] A. Chaubey, P. Konda Gokuldoss, Z. Wang, S. Scudino, N. Mukhopadhyay and J. Eckert, “Effect of Particle Size on Microstructure and Mechanical Properties of Al-Based Composite Reinforced with 10 Vol.% Mechanically Alloyed Mg-7.4%Al Particles,” Technologies, Vol. 4, No. 4, p. 37, (2016). [24] S. Y. Fu, X. Q. Feng, B. Lauke and Y. W. Mai, “Effects of particle size, particle/matrix interface adhesion and particle loading on mechanical properties of particulate-polymer composites,” Compos. Part B Eng., Vol. 39, No. 6, pp. 933–961, (2008). [25] S. Chatterjee, F. Nafezarefi, N. H. Tai, L. Schlagenhauf, F. A. Nüesch and B. T. T. Chu, “Size and synergy effects of nanofiller hybrids including graphene nanoplatelets and carbon nanotubes in mechanical properties of epoxy composites,” Carbon N. Y., Vol. 50, No. 15, pp. 5380–5386, (2012). [26] F. Ross Hallett, “Particle size analysis by dynamic light scattering,” Food Res. Int., Vol. 27, No. 2, pp. 195–198, (1994). [27] B. Krause, M. Mende, P. Pötschke and G. Petzold, “Dispersability and particle size distribution of CNTs in an aqueous surfactant dispersion as a function of ultrasonic treatment time,” Carbon N. Y., Vol. 48, No. 10, pp. 2746–2754, (2010). [28] U. Kätzel, R. Bedrich, M. Stintz, R. Ketzmerick, T. Gottschalk-Gaudig and H. Barthel, “Dynamic light scattering for the characterization of polydisperse fractal systems: I. Simulation of the diffusional behavior,” Part. Part. Syst. Charact., Vol. 25, No. 1, pp. 9–18, (2008). [29] M. Alkan, M. Karadaş, M. Doǧan and Ö. Demirbaş, “Zeta potentials of perlite samples in various electrolyte and surfactant media,” Colloids Surfaces A Physicochem. Eng. Asp., Vol. 259, No. 1–3, pp. 155–166, (2005). [30] H. Nolte, C. Schilde and A. Kwade, “Determination of particle size distributions and the degree of dispersion in nanocomposites,” Compos. Sci. Technol., Vol. 72, No. 9, pp. 948–958, (2012). [31] H. G. Barth and R. B. Flippen, “Particle Size Analysis,” Anal. Chem., Vol. 67, No. 12, pp. 257–272, (1995). [32] R. Pecora, “Dynamic light scattering measurements of nanometer particles in liquids,” J. Nan. Part. Res., Vol. 2, pp. 123–131,(2000). [33] A. Braun, V. Kestens and K. Franks, “A new certified reference material for size analysis of nanoparticles,” J Nanopart Res 14, 1021 (2012). [34] M. De Kanter, “Enabling the measurement of particle sizes in stirred colloidal suspensions by embedding dynamic light scattering into an automated probe head,” Measurement, Vol. 80, pp. 92–98, (2016). [35] C. Zhao, “Enhanced strength in reduced graphene oxide/nickel composites prepared by molecular-level mixing for structural applications,” Appl. Phys. A Mater. Sci. Process., Vol. 118, No. 2, pp. 409–416, (2014). [36] P. Kamalbabu and G. C. M. Kumar, “Effects of Particle Size on Tensile Properties of Marine Coral Reinforced Polymer Composites,” Procedia Mater. Sci., Vol. 5, pp. 802–808, (2014). [37] D. Brown, V. Marcadon, N. D. Albrola and P. Me, “Effect of Filler Particle Size on the Properties of Model Nanocomposites Effect of Filler Particle Size on the Properties of Model Nanocomposites,” Society, Vol. 41, pp. 1499–1511, (2008). [38] J. A. V. Gonçalves, D. A. T. Campos, G. de J. Oliveira, M. de L. da S. Rosa and M. A. Macêdo, “Mechanical properties of epoxy resin based on granite stone powder from the Sergipe fold-and-thrust belt composites,” Mater. Res., Vol. 17, No. 4, pp.878-887,(2014). [39] M. K. Shukla and K. Sharma, “Enhanced Dispersion and Tensile Properties of Graphene / CNT Epoxy Composites by Varying the Filler Ratio,” Int. J. Innov. Technol. Explor. Eng., Vol. 8, No. 4, pp. 103–107, (2019). [40] M. K. Shukla and K. Sharma, “Microstructure and Elemental Investigation of Graphene / CNT Epoxy Composite,” Int. J. Innov. Technol. Explor. Eng., Vol. 8, No. 4, pp. 108–111, (2019). [41] C. A. Schneider, W. S. Rasband and K. W. Eliceiri, “NIH Image to ImageJ: 25 years of image analysis,” Nat. Methods, Vol. 9, No. 7, pp. 671–675, (2012). [42] M. K. Shukla and K. Sharma “Effect of Carbon Nanofillers on the Mechanical and Interfacial Properties of Epoxy Based Nanocomposites: A Review”, Polym. Sci. Ser. A, Vol. 61, pp. 439–460, (2019). [43] M. K. Shukla and K. Sharma, “Improvement in Mechanical and Thermal Properties of Epoxy Hybrid Composites by Functionalized Graphene and Carbon-Nanotubes,” Materials Research Express, Vol. 6, No. 12, pp 125323, (2019). [44] M. K. Shukla and K. Sharma, “Effect of functionalized graphene/ CNT ratio on the synergetic enhancement of mechanical and thermal properties of epoxy hybrid composite,” Materials Research Express, Vol. 6, No. 8, pp 085318, (2019).
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